Us environmental protection agency office of pesticide. Indicates the message appearing in the balance display. Retrieve the calibration weight from the inside of the balance. Indicates the step number in a procedure or a sequence of changes in the balance display. The standard operating procedure is applicable to in process quality assurance areas. If possible, set the balance to read to 5 decimal places. Level the balance, most balances have a stand that is adjustable to meet the proper level, use the bubble as a guide. Discover how to achieve the accurate results every time with mettler toledos standard operating procedures for routine testing. Clean balance pan after each use with a soft brush or damp towel. To outline the procedure for operation of analytical balances in the traces centre and the.
Switch on the main power supply to balance and printer. The precision of the balance should be verified by weighing at least 5 times a weight that is equivalent to approximately 50% of the maximum capacity of the balance. If the instrument is not used according to the manufacturers operating instructions part 1, part 2 and part 3, protection of the instrument may be impaired. Clean up any spillage near by balance and on the balancemounting base by soft brush. Man100 weighing equipment checking and calibration. The 31 weighing design provides two methods of checking the validity of the measurement using an integrated ftest to monitor the. Usps revised chapters 41 and 1251 have new requirements for weighing, including balance calibration and testing. Systematic balance testing minimizes risks and reduces costs. Pick up the checkweight with a forceps, place it carefully on the balance pan, and weigh it. Standard operating procedure operation of analytical balances. Sop on procedure for operation of analytical balance.
Use a mild detergent, di water and lint free wipe if necessary. Close balance doors, if applicable, to reduce draft. Do not use the weighing device for loads less than ten percent of the capacity of the range in use. A satisfactory way of carrying this out is to check the balance for free swing at the tare and loaded position. Weighing by single substitution using a single pan mechanical balance, a full electronic balance, or a balance with digital indications and built in weights may 2019 job aids. Repeat the intermediate weighing of the weight cart as if multiple weights were being verified.
With more than 140 years of experience and quality made in germany, we offer the best weighing option by excelling in speed, repeatability and accuracy. Check that the balance and pans are always kept clean. Balance nonlinearity is a less dominant factor for small mass weighing. If all the parameters fall with the acceptance criteria limit, affix the calibration tag no. Select a weighing device of a lesser capacity for small. It should be emphasised that the daily checks do not obviate the need to check correct operation of the balance each time weighing is carried out. The purpose of the weighing test is to test the accuracy calibrate of the weighing instrument throughout its whole range in several steps, with increasing and decreasing weight. Reference weight set range of 1g to 50g and individual reference weights 1 mg, 10 mg, 100 mg, 100 g, 500 g, 1 kg, 2 kg. Purpose of this sop for operation, cleaning, verification, and calibration of bin lifting trolley with weighing balances. This sop describes the procedure for cleaning a laboratory bench top balance both analytical balance and precision balance. Good weighing practice for lab and production balance.
Auto tare function page 7 i want to tare the balance without waiting for the stability mark to light up. After resetting, calibrate again all the parameters as mentioned in point 6. Qc for analytical balances wisconsin department of. Take the standard weights of different capacity based on the capacity of the balance as. According to the current usp chapter 41, the repeatability part of the test defines the starting point of a balances operating range, which is limited to the maximum capacity of the balance and begins at the point at which the balances repeatability is less than or equal to 0. Sop for operation and calibration of mettler toledo. Auto zero function page 7 i want to automatically tare the balance set the display to zero after outputting a weight reading. Verification of the balance is performed by placing a suitable weight depending on the type of balance in the center of the weighing pan once and comparing the result with predefined acceptance criteria. The latest revisions to the united states pharmacopeia usp general chapters balances and weighing on an analytical balance became official on dec. California environmental protection agency air resources. The balance would do internal calibration automatically, give out the print. Allow to stabilize for 15 to 20 seconds and then select the weight for calibration.
Check that the balance is placed in a draughtfree area and that the pointer is able to swing freely. The same weight should always be used in these verifications. If using an electronic balance, allow to warm up for at least 60 minutes. Officer concerned department is responsible for monthly calibration. Suggested process for verifying analytical balance accuracy and performance 1. Sop 8 or sop 4 to determine the conventional mass value of the weight cart. Check that the pointer is still pointing to the central mark of the scale. Operation and cleaning of electronic weighing balance generation of shipper label pallet label for track and trace system using bar code technology as per sscc code following gsi global standards batch packing. This sop is applicable to the trolley balance in the department at the plant. Standard operating procedure to evaluate the performance of analytical balance used for the analysis in. Weight is measured with a calibrated, electronic digital scale or beam balance. Check the level of balance using built in level indicator. Carefully clean the weighing scale, most weighing scale pans can be removed for better cleaning.
Before calibrating the balance, clean the weighing platforms. If any of the observation is out of limit, correct and reset the balance. This demand specifies the usable weighing range of the. The procedure is operated by trained members of the group who are deemed competent by the operational area manager, metabolic studies. Calibration balance a wide selection of ultramicro, micro, analytical and precision balances allows you to choose any entrylevel to highperformance balance. This sop describes the proper operation of the mettler toledo ab2045 analytical balance in the sobran animal facility. There are many types of laboratory balance but this procedure focuses on electromagnetic balances. The samples are weighed using an appropriate weighing container weighing paper. Sop for operation and calibration of mettler toledo analytical. The electronic scale should be in the kilogram or pound mode as per protocol. Using balances the primary method that you will use to measure the amounts of chemicals is to weigh themthat is, to determine their mass. The balance is again in the weighing mode and ready for operation. This sop describes the optimal use and maintenance of a laboratory balance, i.
The analytical balance is used when weighing small items such as test articles during formulation and animal organs during necropsy. This procedure is applicable for balance installed in the quality control department. Weighing scale calibration how to calibrate weighing. To lay down a procedure for calibration of weighing balances. Before leaving balance the close the glass drafts properly and rezero the balance by pressing. Sartorius analytic balance mn 1712mp8 operating manual version. Used to measure the weight of objects in the laboratory, such as media and reagent ingredients and disinfectant containers. Enter the each weighing process in balance log book.
Anthropometric standardization reference manual by timothy g. Download as docx, pdf, txt or read online from scribd. Analytical balances select a checkweight of an appropriate mass to examine an analytical balance. In cases where calibration is being performed by the balance user, two test weights with a defined mass will be required.
Place identical pieces of greaseproof paper on both pans, if the material to be weighed is a greasy material. Before weighing the first sample of the day, verify the functionaccuracy of the balance by weighing the precision scale weights 1mg, 10mg, and 50mg. Officer production is responsible for verification. This procedure is intended to describe the use of balances in the operational area of metabolic studies. If it is not, press the lbkg key on the keyboard face. It is designed to instruct laboratory personnel on how to proceed for thorough cleaning of a balance. Usp chapter 41 weights and balances has been revised recently in 20 for repeatability and accuracy of weighing balances this usp chapter 41 makes it mandatory for pharmaceutical manufacturers to use use a test weight between 5%. Place weighing container on the balance weighing pan. Title calibration and maintenance of weigh balances.
These revisions aim to ensure weighing accuracy and. Sop on calibration of weighing balance pharmastate blog. Standard operating procedures sops for balance testing. In pharmaceutical industry analytical balance, moisture. Before weighing any filters, verify balance performance by weighing a nist traceable calibration weight 100. Check for batteries for battery operated balances to ensure accurate display and functionality. In such case, measuring result should be corrected according to. How to examine the repeatability of the balance in routine testing. Operating instructions excellence analytical balances xs. If during or before weighing power supply fails, then recalibrate the balance. Before performing weighing assure that, balance is calibrated. You may use this feature by adding opto modules and additional hardware to control filling or loading of cars. Zero tare timing change function page 7 zero point, and taring various weighing methods.
Ensure that balance is kept on a shockproof bench top. This is not a calibration of the balance, it is a verification of calibration. Equipped with a touch screen, it is also suitable for customised workflows qapps. Sop on receipt of raw materials and packaging materials.
Free standard operating procedures consist testing information for lab microbalance, analytical or precision balance on different topics. Follow good laboratory practices such as properly exercising the balance prior to calibration. For mass production balance, balance sensitivity and eccentricity are major factors for consideration. Your balance must provide the same result for repeated weighing of the same load under the same measurement conditions. This sop describes the optimal use and maintenance of a laboratory balance, used to. The specific sop for the double substitution procedure for each balance is to be followed. Check the balance leveling gauge to make sure bubble is inside the target. Routine testing of balances general basic rules for handling balances before using a balance, make sure the balance was left on power for a sufficient period of time mentioned in the balance operating instructions. If the standard deviation obtained is less than ing range and meets the requirements defined for 0. Analytical balances for weighing up to 520 g maximum with 0.